benzyl 2,3,4-tris(benzyloxy)benzoate

Base Information

Chemical Name:benzyl 2,3,4-tris(benzyloxy)benzoate
CAS No.:1609113-44-1
Molecular Formula:C₃₅H₃₀O₅
Molecular Weight:530.62
Hs Code.:

Synonyms:benzyl 2,3,4-tris(benzyloxy)benzoate

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Chemical Property of benzyl 2,3,4-tris(benzyloxy)benzoate

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Technology Process of benzyl 2,3,4-tris(benzyloxy)benzoate

There total 1 articles about benzyl 2,3,4-tris(benzyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 610-02-6
2,3,4-trihydroxybenzoic acid

: 100-39-0
benzyl bromide

: 1609113-44-1
benzyl 2,3,4-tris(benzyloxy)benzoate

Guidance literature:: With potassium carbonate; sodium iodide; In acetone; Reflux;
DOI:10.1039/c4ob00445k

Reference yield: 97.0%

: 1609113-44-1
benzyl 2,3,4-tris(benzyloxy)benzoate

: 180206-32-0
2,3,4-tris(benzyloxy)benzoic acid

Guidance literature:: benzyl 2,3,4-tris(benzyloxy)benzoate; With potassium hydroxide; In methanol; Reflux;

With hydrogenchloride; In methanol; water; at 20 ℃; pH=3 - 4;
DOI:10.1039/c4ob00445k

Reference yield:

: 1609113-44-1
benzyl 2,3,4-tris(benzyloxy)benzoate

: 227026-22-4
N-(2,3,4-trihydroxyphenyl)acetamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydroxide / methanol / Reflux

1.2: 20 °C / pH 3 - 4

2.1: diphenyl phosphoryl azide; triethylamine / 5 h / 20 - 75 °C / Inert atmosphere

3.1: 75 °C

4.1: potassium hydroxide / methanol / 65 °C

5.1: pyridine / 20 °C

6.1: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 25 °C / 2325.23 Torr

With pyridine; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; 2.1: |Curtius Rearrangement;
DOI:10.1039/c4ob00445k