Technology Process of C16H25NO
There total 3 articles about C16H25NO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(S)-2-allyl-2-ethyl-N-benzoyl-δ-valerolactam;
With
sodium periodate;
ruthenium(III) trichloride hydrate;
In
tetrachloromethane; water; acetonitrile;
for 28h;
Inert atmosphere;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 20 - 40 ℃;
for 24h;
With
water;
In
tetrahydrofuran;
at 0 ℃;
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 40 ℃;
Inert atmosphere;
DOI:10.3762/bjoc.10.261
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (S)-2-(2-(bis (4-(Trifluoromethyl)phenyl)phosphino)-5-(trifluoromethyl)phenyl)-4-(tert-butyl)-4,5-dihydrooxazole; Pd(pmdba)2 / toluene / 40 °C / Inert atmosphere
2: ruthenium(III) trichloride hydrate; sodium periodate / water; acetonitrile; tetrachloromethane / Inert atmosphere
3: lithium aluminium tetrahydride / tetrahydrofuran / 40 °C / Inert atmosphere
With
(S)-2-(2-(bis (4-(Trifluoromethyl)phenyl)phosphino)-5-(trifluoromethyl)phenyl)-4-(tert-butyl)-4,5-dihydrooxazole; sodium periodate; lithium aluminium tetrahydride; ruthenium(III) trichloride hydrate; Pd(pmdba)2;
In
tetrahydrofuran; tetrachloromethane; water; toluene; acetonitrile;
DOI:10.3762/bjoc.10.261