4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester

Base Information

• Chemical Name: 4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester
• CAS No.: 64970-85-0
• Molecular Formula: C₂₀H₂₁NO₃S
• Molecular Weight: 355.458

Synonyms:4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester

Chemical Property of 4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester

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Technology Process of 4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester

There total 4 articles about 4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2c-phenyl-thiazolidine-3,4r-dicarboxylic acid 3-methyl ester (64970-79-2) → 4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester (64970-85-0)

Guidance literature:

Multi-step reaction with 3 steps

1: B₂H₆ / tetrahydrofuran / 0.5 h / 25 °C

2: CrO₃, Py / CH₂Cl₂ / 0.25 h

3: tetrahydrofuran / 1.5 h / 25 °C

With pyridine; chromium(VI) oxide; diborane; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00463a042

Reference yield:

(2R,4R)-2-phenyl-1,3-thiazolidine-4-carboxylic acid (64970-78-1) → 4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester (64970-85-0)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. Na₂CO₃, NaHCO₃ / diethyl ether / 1 h / 25 °C

2: B₂H₆ / tetrahydrofuran / 0.5 h / 25 °C

3: CrO₃, Py / CH₂Cl₂ / 0.25 h

4: tetrahydrofuran / 1.5 h / 25 °C

With pyridine; chromium(VI) oxide; sodium hydrogencarbonate; sodium carbonate; diborane; In tetrahydrofuran; diethyl ether; dichloromethane;

DOI:10.1021/ja00463a042

Reference yield:

(2R,4R)-4-hydroxymethyl-2-phenylthiazolidine-3-carboxylic acid methyl ester (64970-80-5) → 4c-(3-methoxy-cis-styryl)-2r-phenyl-thiazolidine-3-carboxylic acid methyl ester (64970-85-0)

Guidance literature:

Multi-step reaction with 2 steps

1: CrO₃, Py / CH₂Cl₂ / 0.25 h

2: tetrahydrofuran / 1.5 h / 25 °C

With pyridine; chromium(VI) oxide; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00463a042

upstream raw materials:

(2R,4R)-2-phenyl-1,3-thiazolidine-4-carboxylic acid

2c-phenyl-thiazolidine-3,4r-dicarboxylic acid 3-methyl ester

(2R,4R)-4-hydroxymethyl-2-phenylthiazolidine-3-carboxylic acid methyl ester

benzaldehyde

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