phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside

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Chemical Name:phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside
CAS No.:205590-25-6
Molecular Formula:C₄₆H₄₄O₁₀S
Molecular Weight:788.915
Hs Code.:

Synonyms:phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside

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Chemical Property of phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside

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Technology Process of phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside

There total 1 articles about phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 100-39-0
benzyl bromide

: 205590-23-4
C₃₉H₃₈O₁₀S

: 205590-25-6
phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside

Guidance literature:: C₃₉H₃₈O₁₀S; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1246/bcsj.71.679

Reference yield: 9.0%

: 108-24-7
acetic anhydride

: 205590-25-6
phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside

: phenyl 4',2'-di-O-acetyl-4,6-O-benzylidene-2,3',6'-tri-O-benzyl-1-thio-β-laminaribioside

: phenyl 2,4,4'-tri-O-acetyl-2',3',6,6'-tetra-O-benzyl-1-thio-β-laminaribioside

Guidance literature:: phenyl 3'-O-benzyl-2,2':4,6:4',6'-tri-O-benzylidene-1-thio-β-laminaribioside; With methanesulfonic acid; 4 A molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; at 20 ℃;

acetic anhydride; With pyridine; at 20 ℃; for 24h;
DOI:10.1246/bcsj.71.679