2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

Base Information

Chemical Name:2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester
CAS No.:870460-71-2
Molecular Formula:C₃₅H₃₄O₅
Molecular Weight:534.652
Hs Code.:

Synonyms:2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

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Chemical Property of 2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

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Technology Process of 2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

There total 2 articles about 2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 93379-48-7
(R,R)-TADDOL

: 920-46-7,26937-45-1
Methacryloyl chloride

: 870460-71-2
2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

: 171979-19-4
(4R,5R)-2,2-dimethyl-α,α,α',α'-tetraphenyl-1,3-dioxolane-4,5-dimethyanol dimethacrylate

Guidance literature:: (R,R)-TADDOL; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃;

Methacryloyl chloride; In tetrahydrofuran; hexane; for 1h; Heating;
DOI:10.1055/s-2005-872123

Reference yield: 65.0%

: 93379-48-7
(R,R)-TADDOL

: 920-46-7,26937-45-1
Methacryloyl chloride

: 870460-71-2
2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

Guidance literature:: (R,R)-TADDOL; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

Methacryloyl chloride; In tetrahydrofuran; hexane; at -78 ℃;
DOI:10.1055/s-2005-872123

Reference yield: 55.0%

: 870460-71-2
2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

: 109-72-8,29786-93-4
n-butyllithium

: 814-68-6,25189-84-8
acryloyl chloride

: 2-Methyl-heptanoic acid [(4R,5R)-5-(acryloyloxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester

Guidance literature:: 2-Methyl-acrylic acid [(4R,5R)-5-(hydroxy-diphenyl-methyl)-2,2-dimethyl-[1,3]dioxolan-4-yl]-diphenyl-methyl ester; n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃;

acryloyl chloride; In tetrahydrofuran; hexane; for 2h; Heating;
DOI:10.1055/s-2005-872123