(E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate

Base Information

Chemical Name:(E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate
CAS No.:952664-63-0
Molecular Formula:C₁₅H₁₇NO₅
Molecular Weight:291.304
Hs Code.:

Synonyms:(E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate

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Chemical Property of (E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate

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Technology Process of (E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate

There total 5 articles about (E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1-[4-hydroxy-3-(1-hydroxyimino-ethyl)-phenyl]-cyclopropanecarboxylic acid methyl ester

: 108-24-7
acetic anhydride

: 952664-63-0
(E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate

Guidance literature:: at 45 ℃; for 4h;

Reference yield: 99.0%

: 1-[4-hydroxy-3-(1-hydroxyimino-ethyl)-phenyl]-cyclopropanecarboxylic methyl ester

: 108-24-7
acetic anhydride

: 952664-63-0
(E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate

Guidance literature:: at 45 ℃; for 4h;

Reference yield:

: 16728-01-1
1-(4-methoxyphenyl)-1-cyclopropanecarboxylic acid

: 952664-63-0
(E)-methyl 1-(3-(1-(acetoxyimino)ethyl)-4-hydroxyphenyl)cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / 20 h / Reflux

2: aluminum (III) chloride / carbon disulfide / 2 h / Reflux

3: sodium acetate; hydroxylamine hydrochloride / ethanol / Reflux

4: 4 h / 45 °C

With aluminum (III) chloride; hydroxylamine hydrochloride; sodium acetate; toluene-4-sulfonic acid; In carbon disulfide; ethanol;