[(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-yl]-methanol

Base Information

• Chemical Name: [(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-yl]-methanol
• CAS No.: 321747-11-9
• Molecular Formula: C₂₂H₂₆O₆
• Molecular Weight: 386.445

Synonyms:[(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-yl]-methanol

Chemical Property of [(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-yl]-methanol

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-yl]-methanol

There total 3 articles about [(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

isolariciresinol dimethyl ether (21966-92-7) → [(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-trien-12-yl]-methanol (321747-11-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; at 25 ℃; for 3h;

DOI:10.1021/jm990563p

Reference yield:

conidendrin (518-55-8,5474-93-1,22614-13-7,26358-20-3,85699-62-3,89104-61-0,105817-20-7) → [(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-trien-12-yl]-methanol (321747-11-9)

Guidance literature:

Multi-step reaction with 3 steps

1: OH^-

2: LAH

3: 48 percent / 2,3-dichloro-5,6-dicyano-1,4-quinone / CH₂Cl₂; tetrahydrofuran / 3 h / 25 °C

With lithium aluminium tetrahydride; hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jm990563p

Reference yield:

α-conidendrin dimethyl ether (71772-18-4) → [(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.02,7]dodeca-2(7),3,5-trien-12-yl]-methanol (321747-11-9)

Guidance literature:

Multi-step reaction with 2 steps

1: LAH

2: 48 percent / 2,3-dichloro-5,6-dicyano-1,4-quinone / CH₂Cl₂; tetrahydrofuran / 3 h / 25 °C

With lithium aluminium tetrahydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane;

DOI:10.1021/jm990563p

upstream raw materials:

isolariciresinol dimethyl ether

conidendrin

α-conidendrin dimethyl ether

Downstream raw materials:

tert-Butyl-[(1S,9R,12R)-1-(3,4-dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-ylmethoxy]-dimethyl-silane

anhydroisolariciresinol dimethyl ether

dimethyl-4-iso-α-conidendrol

isolariciresinol dimethyl ether

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