2-(RS)-phenethylmalonic acid monoethyl ester

Base Information

Chemical Name:2-(RS)-phenethylmalonic acid monoethyl ester
CAS No.:80091-07-2
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:2-(RS)-phenethylmalonic acid monoethyl ester

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Chemical Property of 2-(RS)-phenethylmalonic acid monoethyl ester

Chemical Property:

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Technology Process of 2-(RS)-phenethylmalonic acid monoethyl ester

There total 5 articles about 2-(RS)-phenethylmalonic acid monoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-63-9
1-phenyl-2-bromoethane

: 80091-07-2
2-(RS)-phenethylmalonic acid monoethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOEt / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 50 deg C, 6 h

2: KOH / ethanol / 16 h

With potassium hydroxide; sodium ethanolate; In ethanol;
DOI:10.1021/jm9900164

Reference yield:

: 105-53-3
diethyl malonate

: 80091-07-2
2-(RS)-phenethylmalonic acid monoethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOEt / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 50 deg C, 6 h

2: KOH / ethanol / 16 h

With potassium hydroxide; sodium ethanolate; In ethanol;
DOI:10.1021/jm9900164

Reference yield:

: 103-63-9
1-phenyl-2-bromoethane

: 80091-07-2
2-(RS)-phenethylmalonic acid monoethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium ethanolate / ethanol / 0.92 h / Reflux

1.2: Reflux

2.1: potassium hydroxide / ethanol / 20 °C

2.2: pH 2 - 3

With sodium ethanolate; potassium hydroxide; In ethanol;
DOI:10.1021/jm200438b