1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane

Base Information

Chemical Name:1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane
CAS No.:289665-31-2
Molecular Formula:C₄₃H₄₃P₃
Molecular Weight:652.736
Hs Code.:

Synonyms:1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane

Suppliers and Price of 1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane

There total 1 articles about 1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 29949-64-2
di(o-tolyl)phosphine

: 155932-48-2
methyl(2-methyldiphenylphosphino)-1-chloro-3-diphenylphosphinopropane

: 289665-31-2
1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 130 ℃; for 3h;
DOI:10.1002/(sici)1099-0682(200004)2000:4<597::aid-ejic597>3.0.co;2-7

Reference yield: 67.0%

: 15038-48-9,17731-95-2
tris(acetonitrile)tricarbonylmolybdenum⁽⁰⁾

: 289665-31-2
1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropane

: 289493-55-6
1-[bis(o-tolyl)phosphanyl]-3-(diphenylphosphanyl)-2-(diphenylphosphanylmethyl)-2-methylpropanetricarbonylmolybdenum

Guidance literature:: In dichloromethane; to soln. of ligand in CH2Cl2 solid Mo-complex was added, mixt. was stirred for 2 h at room temp.; solvent was removed, column chromy. (silica gel, petroleum ether/CH2Cl2), recrystd. from CH2Cl2;
DOI:10.1002/(sici)1099-0682(200004)2000:4<597::aid-ejic597>3.0.co;2-7