4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide

Base Information

Chemical Name:4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide
CAS No.:1238700-81-6
Molecular Formula:C₁₂H₉F₃N₄O₂
Molecular Weight:298.224
Hs Code.:

Synonyms:4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide

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Chemical Property of 4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide

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Technology Process of 4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide

There total 1 articles about 4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 478063-65-9
methyl 4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carboxylate

: 1238700-81-6
4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; at 120 ℃; for 0.166667h; Microwave irradiation;

Reference yield: 53.0%

: 1238700-81-6
4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 62-53-3
aniline

: 1238695-16-3
3-(4-phenyl-4H-1,2,4-triazol-3-yl)-1-[3-(trifluoromethyl)phenyl]pyridazin-4(1H)-one

Guidance literature:: 4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide; N,N-dimethyl-formamide dimethyl acetal; In acetonitrile; at 55 ℃; for 0.75h;

aniline; With acetic acid; In acetonitrile; at 125 ℃; for 2h;

Reference yield: 46.0%

: 18871-66-4
N,N-dimethylacetamide dimethyl acetal

: 1238700-81-6
4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide

: 62-53-3
aniline

: 1238695-20-9
3-(5-methyl-4-phenyl-4H-1,2,4-triazol-3-yl)-1-[3-(trifluoromethyl)phenyl]pyridazin-4(1H)-one

Guidance literature:: N,N-dimethylacetamide dimethyl acetal; 4-oxo-1-[3-(trifluoromethyl)phenyl]-1,4-dihydropyridazine-3-carbohydrazide; In acetonitrile; at 60 ℃; for 2.5h;

aniline; With acetic acid; In acetonitrile; at 125 ℃; for 2h;