3-amino-5-aminomethylbenzoic acid

Base Information

Chemical Name:3-amino-5-aminomethylbenzoic acid
CAS No.:30713-31-6
Molecular Formula:C₈H₁₀N₂O₂
Molecular Weight:166.18
Hs Code.:

Synonyms:3-amino-5-aminomethylbenzoic acid

Suppliers and Price of 3-amino-5-aminomethylbenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-amino-5-aminomethylbenzoic acid

Chemical Property:

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Technology Process of 3-amino-5-aminomethylbenzoic acid

There total 10 articles about 3-amino-5-aminomethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1452402-92-4
3-amino-5-(azidomethyl)benzoic acid

: 30713-31-6
3-amino-5-aminomethylbenzoic acid

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; acetic acid; for 72h;
DOI:10.3762/bjoc.10.49

Reference yield:

: 220286-47-5
3-Amino-5-hydroxymethylbenzoic acid methyl ester

: 30713-31-6
3-amino-5-aminomethylbenzoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / tetrahydrofuran / 6 h / 20 °C

2.1: pyridine; thionyl chloride / dichloromethane / 0 - 20 °C

3.1: sodium azide / water; acetone / Reflux

4.1: lithium hydroxide / methanol; water / 4 h / 55 °C

4.2: pH 2

5.1: hydrogenchloride / water / Reflux

5.2: pH 5

6.1: palladium on activated charcoal; hydrogen / methanol; acetic acid / 72 h

With pyridine; hydrogenchloride; thionyl chloride; sodium azide; palladium on activated charcoal; hydrogen; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid; acetone;
DOI:10.3762/bjoc.10.49

Reference yield:

: 1160157-92-5
methyl 3-(acetylamino)-5-(hydroxymethyl)benzoate

: 30713-31-6
3-amino-5-aminomethylbenzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine; thionyl chloride / dichloromethane / 0 - 20 °C

2.1: sodium azide / water; acetone / Reflux

3.1: lithium hydroxide / methanol; water / 4 h / 55 °C

3.2: pH 2

4.1: hydrogenchloride / water / Reflux

4.2: pH 5

5.1: palladium on activated charcoal; hydrogen / methanol; acetic acid / 72 h

With pyridine; hydrogenchloride; thionyl chloride; sodium azide; palladium on activated charcoal; hydrogen; lithium hydroxide; In methanol; dichloromethane; water; acetic acid; acetone;
DOI:10.3762/bjoc.10.49