[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COMe)2-P,P')]PF₆

Base Information

• Chemical Name: [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COMe)2-P,P')]PF₆
• CAS No.: 494831-14-0
• Molecular Formula: C₄₆H₅₀NO₄P₂Pd*F₆P
• Molecular Weight: 994.239
• Mol file: 494831-14-0.mol

Synonyms:[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COMe)2-P,P')]PF₆

Chemical Property of [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COMe)2-P,P')]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COMe)2-P,P')]PF₆

There total 1 articles about [Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CHCH₂CH(COMe)2-P,P')]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

[Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)((Ph2P)2CCH2-P,P')]PF6 (494831-09-3) + acetylacetone (123-54-6,81235-32-7) → [Pd(2,3-(MeO)2C6H2CH=N(Cy)-C6,N)((Ph2P)2CHCH2CH(COMe)2-P,P')]PF6 (494831-14-0)

Guidance literature:

sodium carbonate; In chloroform; under Ar, 2 equiv. of acetylacetone, heating in dry CHCl3 at 45 °C for 2 h in the presence of anhyd. Na2CO3; soln. was cooled to room temp., filtered through Celite, evapd. in vac.,residue was triturated with Et2O, filtered off, washed with cold Et2O, dried in vac.;

DOI:10.1039/b203864a

upstream raw materials:

[Pd(2,3-(MeO)2C₆H₂CH=N(Cy)-C₆,N)((Ph₂P)2CCH₂-P,P')]PF₆

acetylacetone