C₆₂H₇₁N₁₅O₁₁S₆Si

Base Information

Chemical Name:C₆₂H₇₁N₁₅O₁₁S₆Si
CAS No.:946851-43-0
Molecular Formula:C₆₂H₇₁N₁₅O₁₁S₆Si
Molecular Weight:1422.82
Hs Code.:

C<sub>62</sub>H<sub>71</sub>N<sub>15</sub>O<sub>11</sub>S<sub>6</sub>Si

Synonyms:C₆₂H₇₁N₁₅O₁₁S₆Si

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Chemical Property of C₆₂H₇₁N₁₅O₁₁S₆Si

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Technology Process of C₆₂H₇₁N₁₅O₁₁S₆Si

There total 18 articles about C₆₂H₇₁N₁₅O₁₁S₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 946851-37-2
C₂₆H₃₉N₅O₇S₂

: 946851-43-0
C₆₂H₇₁N₁₅O₁₁S₆Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: ethanol / 0 - 25 °C

2.1: N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride; 1-hydroxybenzotriazole / dimethylformamide / 16 h / -10 - 25 °C

3.1: 87 percent / tri(2-furyl)phosphate / Pd₂(dibenzylideneacetone)3 / tetrahydrofuran; N,N-dimethyl-acetamide / 16 h / 45 °C

4.1: 48 percent / PdCl₂(PPh₃)2 / N,N-dimethyl-acetamide / 3.5 h / 45 °C

5.1: aq. LiOH / 2-methyl-propan-2-ol; tetrahydrofuran / 1 h / 25 °C

6.1: diphenylphosphoryl azide; iPr₂NEt / dimethylformamide / 16 h / 25 °C

6.2: Pd(PPh₃)4 / toluene / 85 °C

7.1: trifluoroacetic acid / CH₂Cl₂ / 2 h / 25 °C

8.1: iPr₂NEt; TOTU / dimethylformamide / 4 h / 25 °C

With lithium hydroxide; O-[(ethoxycarbonyl)cyanomethyleneamino]-N,N,N',N'-tetramethyluronium tetrafluoroborate; diphenylphosphoranyl azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Negishi cross-coupling reaction / 4.1: Negishi cross-coupling reaction / 6.1: Stille coupling reaction;
DOI:10.1002/anie.200700684

Reference yield:

: 946851-34-9
C₂₅H₃₁N₆O₆S₃I

: 946851-43-0
C₆₂H₇₁N₁₅O₁₁S₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 87 percent / tri(2-furyl)phosphate / Pd₂(dibenzylideneacetone)3 / tetrahydrofuran; N,N-dimethyl-acetamide / 16 h / 45 °C

2.1: 48 percent / PdCl₂(PPh₃)2 / N,N-dimethyl-acetamide / 3.5 h / 45 °C

3.1: aq. LiOH / 2-methyl-propan-2-ol; tetrahydrofuran / 1 h / 25 °C

4.1: diphenylphosphoryl azide; iPr₂NEt / dimethylformamide / 16 h / 25 °C

4.2: Pd(PPh₃)4 / toluene / 85 °C

5.1: trifluoroacetic acid / CH₂Cl₂ / 2 h / 25 °C

6.1: iPr₂NEt; TOTU / dimethylformamide / 4 h / 25 °C

With lithium hydroxide; O-[(ethoxycarbonyl)cyanomethyleneamino]-N,N,N',N'-tetramethyluronium tetrafluoroborate; diphenylphosphoranyl azide; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Negishi cross-coupling reaction / 2.1: Negishi cross-coupling reaction / 4.1: Stille coupling reaction;
DOI:10.1002/anie.200700684

Reference yield:

: C₂₃H₃₃N₅O₆S₂

: 946851-43-0
C₆₂H₇₁N₁₅O₁₁S₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride; 1-hydroxybenzotriazole / dimethylformamide / 16 h / -10 - 25 °C

2.1: 87 percent / tri(2-furyl)phosphate / Pd₂(dibenzylideneacetone)3 / tetrahydrofuran; N,N-dimethyl-acetamide / 16 h / 45 °C

3.1: 48 percent / PdCl₂(PPh₃)2 / N,N-dimethyl-acetamide / 3.5 h / 45 °C

4.1: aq. LiOH / 2-methyl-propan-2-ol; tetrahydrofuran / 1 h / 25 °C

5.1: diphenylphosphoryl azide; iPr₂NEt / dimethylformamide / 16 h / 25 °C

5.2: Pd(PPh₃)4 / toluene / 85 °C

6.1: trifluoroacetic acid / CH₂Cl₂ / 2 h / 25 °C

7.1: iPr₂NEt; TOTU / dimethylformamide / 4 h / 25 °C

With lithium hydroxide; O-[(ethoxycarbonyl)cyanomethyleneamino]-N,N,N',N'-tetramethyluronium tetrafluoroborate; diphenylphosphoranyl azide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide; tert-butyl alcohol; 2.1: Negishi cross-coupling reaction / 3.1: Negishi cross-coupling reaction / 5.1: Stille coupling reaction;
DOI:10.1002/anie.200700684