7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine

Base Information

Chemical Name:7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine
CAS No.:850532-56-8
Molecular Formula:C₃₅H₃₀FNO₄S
Molecular Weight:579.692
Hs Code.:

7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2<i>H</i>-benzo[1,4]oxazine

Synonyms:7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine

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Chemical Property of 7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine

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Technology Process of 7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine

There total 5 articles about 7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 785805-47-2
N-(2,4-difluorophenyl)-N-[(2S)-3-triphenylmethyloxy-2-hydroxypropyl]-4-methylbenzenesulfonamide

: 850532-56-8
7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 1h; Heating;
DOI:10.1016/j.bmc.2004.07.048

Reference yield:

: 367-25-9,76563-56-9
2,4-difluorophenylamine

: 850532-56-8
7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / CH₂Cl₂

2: 100 percent / K₂CO₃; BnEt₃NCl / dioxane

3: t-BuOK / tetrahydrofuran

With pyridine; potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2004.07.039

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 850532-56-8
7-fluoro-4-(toluene-4-sulfonyl)-2-trityloxymethyl-3,4-dihydro-2H-benzo[1,4]oxazine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / CH₂Cl₂

2: 100 percent / K₂CO₃; BnEt₃NCl / dioxane

3: t-BuOK / tetrahydrofuran

With pyridine; potassium tert-butylate; N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.bmcl.2004.07.039