4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

Base Information

Chemical Name:4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine
CAS No.:79974-62-2
Molecular Formula:C₂₈H₃₁N₅O₅
Molecular Weight:517.585
Hs Code.:

Synonyms:4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

Suppliers and Price of 4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Pictogram(s):
Hazard Codes:

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Technology Process of 4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

There total 1 articles about 4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150-61-8
N,N'-diphenylethylenediamine

: 16667-80-4
2',3'-O-isopropylidene-N⁴-acetylcytidine

: 79974-62-2
4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

Guidance literature:: With pyridine; acetic acid; dicyclohexyl-carbodiimide; trifluoroacetic acid; Yield given. Multistep reaction; 1.) DMSO, H₂O, RT, 30 min, 2.) MeOH, 1 h;

Reference yield:

: 79974-62-2
4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

: 2595-97-3
D-Allose

Guidance literature:: Multi-step reaction with 4 steps

1: Dowex 50 resin (H⁺) / trifluoroacetic acid; H₂O / 1 h / Ambient temperature

2: 38 percent / tetrahydrofuran / 2 h / 60 °C

3: 28 percent / boron trifluoride-ether / tetrahydrofuran / 0.08 h / Ambient temperature

4: Dowex 50 resin (H⁺) / H₂O / 1.5 h / 100 °C

With Dowex 50 resin (H⁺); boron trifluoride diethyl etherate; In tetrahydrofuran; water; trifluoroacetic acid;

Reference yield:

: 79974-62-2
4-N-acetyl-1-<5-deoxy-2,3-O-isopropylidene-5,5-(N,N'-diphenylethylenediamino)-β-D-ribofuranosyl>cytosine

: 23567-25-1
L-(?)-talose

Guidance literature:: Multi-step reaction with 4 steps

1: Dowex 50 resin (H⁺) / trifluoroacetic acid; H₂O / 1 h / Ambient temperature

2: 38 percent / tetrahydrofuran / 2 h / 60 °C

3: 65 percent / boron trifluoride-ether / tetrahydrofuran / 0.08 h / Ambient temperature

4: Dowex 50 resin (H⁺) / H₂O / 1.5 h / 100 °C

With Dowex 50 resin (H⁺); boron trifluoride diethyl etherate; In tetrahydrofuran; water; trifluoroacetic acid;