(2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester

Base Information

Chemical Name:(2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester
CAS No.:1372937-20-6
Molecular Formula:C₃₅H₃₇NO₄
Molecular Weight:535.683
Hs Code.:

Synonyms:(2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester

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Chemical Property of (2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester

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Technology Process of (2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester

There total 4 articles about (2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 611-99-4
4,4'-Dihydroxybenzophenone

: 1372937-20-6
(2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 48 h / 60 °C

2: zinc; titanium tetrachloride / tetrahydrofuran / 18 h / -10 - 80 °C

3: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 70 °C

With titanium tetrachloride; potassium carbonate; caesium carbonate; zinc; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; 2: McMurry Reaction;

Reference yield:

: 25450-10-6
2-[N-(ethyloxycarbonyl)-N-methylamino]ethanol

: 1372937-20-6
(2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 1 h / 0 - 20 °C

2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 70 °C

With 1H-imidazole; iodine; caesium carbonate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 94972-95-9
4-hydroxy-4'-benzyloxybenzophenone

: 1372937-20-6
(2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; titanium tetrachloride / tetrahydrofuran / 18 h / -10 - 80 °C

2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 70 °C

With titanium tetrachloride; caesium carbonate; zinc; In tetrahydrofuran; N,N-dimethyl-formamide; 1: McMurry Reaction;