Technology Process of (2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester
There total 4 articles about (2-(4-(1-(4-benzyloxyphenyl)-2-phenylbut-1-enyl)phenyloxy)ethyl)methylcarbamic acid ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetone / 48 h / 60 °C
2: zinc; titanium tetrachloride / tetrahydrofuran / 18 h / -10 - 80 °C
3: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 70 °C
With
titanium tetrachloride; potassium carbonate; caesium carbonate; zinc;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone;
2: McMurry Reaction;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 1 h / 0 - 20 °C
2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 70 °C
With
1H-imidazole; iodine; caesium carbonate; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: zinc; titanium tetrachloride / tetrahydrofuran / 18 h / -10 - 80 °C
2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 - 70 °C
With
titanium tetrachloride; caesium carbonate; zinc;
In
tetrahydrofuran; N,N-dimethyl-formamide;
1: McMurry Reaction;
