Technology Process of 5-benzoyl-3-carboxymethylbenzothiophene
There total 7 articles about 5-benzoyl-3-carboxymethylbenzothiophene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium dichromate;
In
acetic acid;
at 100 - 105 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) 10percent sodium carbonate; 2.) 40percent sodium hydroxide / 1.) water, 80 deg C, 30 min; 2) 1.5 h, water bath
2: 68 percent / 0.33 h / 290 °C
3: 81.6 percent / sulfuric acid / 6 h / Heating
4: 86 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 7 h / Heating
5: 69.7 percent / aluminum chloride / CS2 / 2 h / -15 - -10 °C
6: 56 percent / K2Cr2O7 / acetic acid / 16 h / 100 - 105 °C
With
potassium dichromate; sodium hydroxide; N-Bromosuccinimide; sulfuric acid; sodium carbonate; dibenzoyl peroxide;
aluminium trichloride;
In
carbon disulfide; tetrachloromethane; acetic acid;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 81.6 percent / sulfuric acid / 6 h / Heating
2: 86 percent / N-bromosuccinimide, dibenzoyl peroxide / CCl4 / 7 h / Heating
3: 69.7 percent / aluminum chloride / CS2 / 2 h / -15 - -10 °C
4: 56 percent / K2Cr2O7 / acetic acid / 16 h / 100 - 105 °C
With
potassium dichromate; N-Bromosuccinimide; sulfuric acid; dibenzoyl peroxide;
aluminium trichloride;
In
carbon disulfide; tetrachloromethane; acetic acid;
