allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside

Base Information

Chemical Name:allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside
CAS No.:327594-00-3
Molecular Formula:C₄₃H₄₆O₁₁
Molecular Weight:738.832
Hs Code.:

Synonyms:allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside

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Chemical Property of allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside

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Technology Process of allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside

There total 4 articles about allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 327593-89-5
allyl 3-O-benzyl-α-L-fucopyranoside

: 327593-98-6
C₂₇H₂₅BrO₆

: 327594-00-3
allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside

Guidance literature:: allyl 3-O-benzyl-α-L-fucopyranoside; With 4 A molecular sieve; mercury(II) cyanide; mercury dibromide; In dichloromethane; at 20 ℃; for 0.75h;

C₂₇H₂₅BrO₆; In dichloromethane; for 10h;
DOI:10.1080/07328300008544140

Reference yield:

: 100-39-0
benzyl bromide

: 327594-00-3
allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: Bu₂SnO / toluene / Heating

1.2: 30 percent / Bu₄NBr / toluene / 3 h / Heating

2.1: Hg(CN)2; HgBr₂; molecular sieves 4A / CH₂Cl₂ / 0.75 h / 20 °C

2.2: 216 mg / CH₂Cl₂ / 10 h

With 4 A molecular sieve; mercury(II) cyanide; di(n-butyl)tin oxide; mercury dibromide; In dichloromethane; toluene;
DOI:10.1080/07328300008544140

Reference yield:

: 41308-77-4
allyl α-L-fucopyranoside

: 327594-00-3
allyl 2-O-(3,4-di-O-benzoyl-2-O-benzyl-α-L-fucopyranosyl)-3-O-benzyl-α-L-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: Bu₂SnO / toluene / Heating

1.2: 30 percent / Bu₄NBr / toluene / 3 h / Heating

2.1: Hg(CN)2; HgBr₂; molecular sieves 4A / CH₂Cl₂ / 0.75 h / 20 °C

2.2: 216 mg / CH₂Cl₂ / 10 h

With 4 A molecular sieve; mercury(II) cyanide; di(n-butyl)tin oxide; mercury dibromide; In dichloromethane; toluene;
DOI:10.1080/07328300008544140