C₄₁H₄₈O₇

Base Information

Chemical Name:C₄₁H₄₈O₇
CAS No.:1421916-98-4
Molecular Formula:C₄₁H₄₈O₇
Molecular Weight:652.828
Hs Code.:

C<sub>41</sub>H<sub>48</sub>O<sub>7</sub>

Synonyms:C₄₁H₄₈O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₁H₄₈O₇

Chemical Property:

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Technology Process of C₄₁H₄₈O₇

There total 15 articles about C₄₁H₄₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₁H₅₀O₇

: 1421916-98-4
C₄₁H₄₈O₇

Guidance literature:: With Jones reagent; In acetone; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1016/j.steroids.2012.10.021

Reference yield:

: 227178-66-7
3β-acetoxy-12β-hydroxy-5α-spirostan-14-ene

: 1421916-98-4
C₄₁H₄₈O₇

Guidance literature:: Multi-step reaction with 11 steps

1: pyridine / 6 h / Inert atmosphere

2: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 19 h / 0 - 25 °C / Inert atmosphere

3: triphenylphosphine; 1H-imidazole; iodine / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

4: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere

5: hydroquinidein 1,4-phthalazinediyl diether; potassium carbonate; potassium hexacyanoferrate(III); potassium osmate(VI) / water; tert-butyl alcohol / 18 h / 0 °C / Inert atmosphere

6: 1H-imidazole; dmap / dichloromethane / 1 h / 25 °C / Inert atmosphere

7: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere

8: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere

9: iodine; [bis(acetoxy)iodo]benzene / dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

10: potassium carbonate / methanol; water / 12 h / 25 °C / Inert atmosphere

11: Jones reagent / acetone / 0.33 h / 0 °C / Inert atmosphere

With pyridine; 1H-imidazole; triethylsilane; dmap; potassium osmate(VI); Jones reagent; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; iodine; potassium carbonate; magnesium dibromide etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene; hydroquinidein 1,4-phthalazinediyl diether; triethylamine; triphenylphosphine; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1016/j.steroids.2012.10.021

Reference yield:

: C₄₂H₆₄O₇Si

: 1421916-98-4
C₄₁H₄₈O₇

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; magnesium dibromide etherate / dichloromethane / 2 h / 25 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 1 h / Inert atmosphere

3: iodine; [bis(acetoxy)iodo]benzene / dichloromethane; cyclohexane / 6 h / 0 °C / Inert atmosphere

4: potassium carbonate / methanol; water / 12 h / 25 °C / Inert atmosphere

5: Jones reagent / acetone / 0.33 h / 0 °C / Inert atmosphere

With Jones reagent; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; iodine; potassium carbonate; magnesium dibromide etherate; triethylamine; In methanol; dichloromethane; cyclohexane; water; acetone;
DOI:10.1016/j.steroids.2012.10.021