3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide

Base Information

Chemical Name:3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide
CAS No.:1286795-95-6
Molecular Formula:C₂F₆NO₄S₂*C₁₆H₂₃N₂O
Molecular Weight:539.52
Hs Code.:

Synonyms:3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide

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Technology Process of 3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide

There total 7 articles about 3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1176198-82-5
1-(4-methoxyphenyl)-3-hexyl-1H-imidazolium bromide

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1286795-95-6
3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide

Guidance literature:: In dichloromethane; water; at 20 ℃;
DOI:10.1002/asia.201000744

Reference yield: 93.0%

: 3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium iodide

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1286795-95-6
3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide

Guidance literature:: In methanol; dichloromethane; water; at 20 ℃; for 12h;
DOI:10.1002/chem.201601063

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1286795-95-6
3-hexyl-1-(4-methoxyphenyl)-1H-imidazol-3-ium bis(trifluoromethylsulfonyl)imide

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol; water / 20 °C

2.1: ammonium chloride / methanol; water / 1 h / Reflux

2.2: 4 h / Reflux

2.3: pH 9

3.1: tetrahydrofuran / 20 h / 95 °C / pressure tube

4.1: dichloromethane; water / 20 °C

With ammonium chloride; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/asia.201000744