C₃₈H₃₀O₁₀S₂

Base Information

Chemical Name:C₃₈H₃₀O₁₀S₂
CAS No.:1033736-90-1
Molecular Formula:C₃₈H₃₀O₁₀S₂
Molecular Weight:710.782
Hs Code.:

C<sub>38</sub>H<sub>30</sub>O<sub>10</sub>S<sub>2</sub>

Synonyms:C₃₈H₃₀O₁₀S₂

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Chemical Property of C₃₈H₃₀O₁₀S₂

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Technology Process of C₃₈H₃₀O₁₀S₂

There total 6 articles about C₃₈H₃₀O₁₀S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1033736-44-5
(4-oxo-3-phenyl-4H-1,1-dioxothiochromen-2-yl)methyl chloroformate

: 1033736-93-4
4-hydroxybutyl (4-oxo-3-phenyl-4H-thiochromen-2-yl)methylcarbonate

: 1033736-90-1
C₃₈H₃₀O₁₀S₂

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃;

Reference yield:

: 771-40-4
2-methyl-4H-thiochromen-4-one

: 1033736-90-1
C₃₈H₃₀O₁₀S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: iodine; cerium(IV)diammonium nitrate / acetonitrile / 4 h / 60 °C / Inert atmosphere

2.1: potassium carbonate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 4 h / 80 °C / Inert atmosphere

3.1: selenium(IV) oxide / chlorobenzene / 12 h / Reflux; Inert atmosphere

3.2: 2 h / 0 °C / Inert atmosphere

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 8 h / 20 °C

5.1: toluene; tetrahydrofuran / 0 - 20 °C

6.1: pyridine / dichloromethane / 0 - 20 °C

With pyridine; selenium(IV) oxide; cerium(IV)diammonium nitrate; iodine; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; chlorobenzene; toluene; acetonitrile;

Reference yield:

: 140173-38-2
3-iodo-2-methyl-4H-benzothiopyran-4-one

: 1033736-90-1
C₃₈H₃₀O₁₀S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 4 h / 80 °C / Inert atmosphere

2.1: selenium(IV) oxide / chlorobenzene / 12 h / Reflux; Inert atmosphere

2.2: 2 h / 0 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 8 h / 20 °C

4.1: toluene; tetrahydrofuran / 0 - 20 °C

5.1: pyridine / dichloromethane / 0 - 20 °C

With pyridine; selenium(IV) oxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; chlorobenzene; toluene;