(E)-N-methyl-2,3-diphenylacrylamide

Base Information

Chemical Name:(E)-N-methyl-2,3-diphenylacrylamide
CAS No.:32175-25-0
Molecular Formula:C₁₆H₁₅NO
Molecular Weight:237.301
Hs Code.:

Synonyms:(E)-N-methyl-2,3-diphenylacrylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-methyl-2,3-diphenylacrylamide

Chemical Property:

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Technology Process of (E)-N-methyl-2,3-diphenylacrylamide

There total 4 articles about (E)-N-methyl-2,3-diphenylacrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: (E)-N-(2,3-diphenylacryloyl)-N-methylbenzamide

: 32175-25-0
(E)-N-methyl-2,3-diphenylacrylamide

Guidance literature:: With sodium hydroxide; In methanol; for 6h; Reflux;
DOI:10.1021/acs.orglett.0c02099

Reference yield:

: 91-48-5
(E)-2,3-diphenylpropenoic acid

: 32175-25-0
(E)-N-methyl-2,3-diphenylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / dichloromethane / 0 - 20 °C / Inert atmosphere

2: dichloromethane / 20 °C / Inert atmosphere

With N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1002/anie.201306754

Reference yield:

: 886-38-4
diphenylcyclopropenone

: 32175-25-0
(E)-N-methyl-2,3-diphenylacrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: silver trifluoromethanesulfonate / 1,2-dimethoxyethane / 0.5 h / 100 °C / Inert atmosphere

2: sodium hydroxide / methanol / 6 h / Reflux

With silver trifluoromethanesulfonate; sodium hydroxide; In methanol; 1,2-dimethoxyethane;
DOI:10.1021/acs.orglett.0c02099