6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

Base Information

Chemical Name:6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane
CAS No.:147067-16-1
Molecular Formula:C₁₉H₃₀O₇S
Molecular Weight:402.509
Hs Code.:

Synonyms:6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

Suppliers and Price of 6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

There total 7 articles about 6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 98-59-9
p-toluenesulfonyl chloride

: 147067-15-0
6-hydroxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

: 147067-16-1
6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

Guidance literature:: With pyridine; at 4 ℃;

Reference yield:

: 92144-75-7
3,7-dioxanonane-1,9-diylbis(toluene-p-sulphonate)

: 147067-16-1
6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / LiBr, t-BuOLi / 2-methyl-propan-2-ol / 108 h / 60 °C

2: 91 percent / toluene-p-sulfonic acid, H₂ / Pd(OH)2/C / ethanol / 48 h / 25 °C / 2280 Torr

3: 54 percent / pyridine / 96 h / -20 °C

With pyridine; hydrogen; toluene-4-sulfonic acid; lithium bromide; lithium tert-butoxide; palladium dihydroxide; In ethanol; tert-butyl alcohol;

Reference yield:

: 4270-73-9
2-methyl-2-<(benzyloxy)methyl>-1,3-propanediol

: 147067-16-1
6-toluene-p-sulfonyloxymethyl-6-methyl-1,4,8,11-tetraoxacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / LiBr, t-BuOLi / 2-methyl-propan-2-ol / 108 h / 60 °C

2: 91 percent / toluene-p-sulfonic acid, H₂ / Pd(OH)2/C / ethanol / 48 h / 25 °C / 2280 Torr

3: 54 percent / pyridine / 96 h / -20 °C

With pyridine; hydrogen; toluene-4-sulfonic acid; lithium bromide; lithium tert-butoxide; palladium dihydroxide; In ethanol; tert-butyl alcohol;