C₇₇H₅₀

Base Information

Chemical Name:C₇₇H₅₀
CAS No.:1158844-49-5
Molecular Formula:C₇₇H₅₀
Molecular Weight:975.244
Hs Code.:

Synonyms:C₇₇H₅₀

Suppliers and Price of C₇₇H₅₀

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₇₇H₅₀

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₇₇H₅₀

There total 10 articles about C₇₇H₅₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1158844-84-8
C₄₉H₄₈B₂O₄

: 23674-20-6
9-bromo-10-phenylanthracene

: 1158844-49-5
C₇₇H₅₀

Guidance literature:: With Aliquat 336; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; toluene; at 100 ℃; for 4h;

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1158844-49-5
C₇₇H₅₀

Guidance literature:: Multi-step reaction with 6 steps

1.1: magnesium / diethyl ether / 4 h / Reflux

1.2: 12 h / Reflux

2.1: trifluorormethanesulfonic acid / Heating

3.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / toluene; ethanol; water / 12 h / 100 °C

4.1: bromine / dichloromethane / -5 - 25 °C

5.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C

5.2: -78 - 25 °C

6.1: potassium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 4 h / 100 °C

With n-butyllithium; trifluorormethanesulfonic acid; bromine; Aliquat 336; sodium carbonate; potassium carbonate; magnesium; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; toluene;

Reference yield:

: 98-80-6
phenylboronic acid

: 1158844-49-5
C₇₇H₅₀

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / toluene; ethanol; water / 12 h / Reflux

2: N-Bromosuccinimide / dichloromethane / 5 h / 20 °C

3: potassium carbonate; Aliquat 336 / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / 4 h / 100 °C

With N-Bromosuccinimide; Aliquat 336; sodium carbonate; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; water; toluene;