(4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide

Base Information

Chemical Name:(4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide
CAS No.:145063-86-1
Molecular Formula:C₂₆H₃₅NO₂
Molecular Weight:393.569
Hs Code.:

Synonyms:(4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide

Chemical Property:

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Technology Process of (4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide

There total 2 articles about (4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 145063-85-0
(2S,3R,4S,5S)-5-dibenzylamino-3-fluorodimethylsilyl-2-isopropyl-7-methyl-4-octanolide

: 145063-86-1
(4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide

Guidance literature:: With triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; for 15h; Ambient temperature;
DOI:10.1055/s-1992-26248

Reference yield:

: 145064-00-2
(2S,3R,4S,5S)-5-dibenzylamino-3-dimethylphenylsilyl-2-isopropyl-7-methyl-4-octanolide

: 145063-86-1
(4E)-5-dibenzyl-3-hydroxy-2-isopropyl-7-methyl-4-octenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 54percent HBF₄ / CH₂Cl₂; diethyl ether / 6 h / Ambient temperature

2: 57 percent / 3-chloroperbenzoic acid, Et₃N / diethyl ether / 15 h / Ambient temperature

With tetrafluoroboric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane;
DOI:10.1055/s-1992-26248