tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane

Base Information

Chemical Name:tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane
CAS No.:181936-01-6
Molecular Formula:C₂₆H₃₆O₃Si
Molecular Weight:424.656
Hs Code.:

Synonyms:tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane

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Chemical Property of tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane

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Technology Process of tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane

There total 5 articles about tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 181935-98-8
1-{3-[1-(4-Methoxy-benzyloxy)-ethyl]-phenyl}-but-3-yn-1-ol

: 181936-01-6
tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 1h; Ambient temperature;
DOI:10.1016/0040-4020(96)00667-9

Reference yield:

: 2746-25-0
p-Methoxybenzyl bromide

: 181936-01-6
tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 0 deg C, 1 h, 2.) DMF, 0 deg C, 1 h

2: 89 percent / SiO₂, 1percent H₂SO₄ / CH₂Cl₂ / 1 h

3: 88 percent / Al, HgCl₂ / tetrahydrofuran / 0.5 h / Ambient temperature

4: 94 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

With 1H-imidazole; sulfuric acid; silica gel; sodium hydride; aluminium; mercury dichloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00667-9

Reference yield:

: 181933-87-9
2-(3'-dimethoxymethyl)phenyl-ethan-2-ol

: 181936-01-6
tert-Butyl-(1-{3-[1-(4-methoxy-benzyloxy)-ethyl]-phenyl}-but-3-ynyloxy)-dimethyl-silane

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 0 deg C, 1 h, 2.) DMF, 0 deg C, 1 h

2: 89 percent / SiO₂, 1percent H₂SO₄ / CH₂Cl₂ / 1 h

3: 88 percent / Al, HgCl₂ / tetrahydrofuran / 0.5 h / Ambient temperature

4: 94 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

With 1H-imidazole; sulfuric acid; silica gel; sodium hydride; aluminium; mercury dichloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(96)00667-9