N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine

Base Information

Chemical Name:N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine
CAS No.:1224570-47-1
Molecular Formula:C₁₇H₂₁Cl₂N₅O₃
Molecular Weight:414.291
Hs Code.:

Synonyms:N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine

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Technology Process of N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine

There total 2 articles about N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 857672-28-7
1-isopropyl-2-methylsulfanyl-1H-imidazole-4,5-dione

: 1224570-72-2
N-(t-butyloxy)-N'-(3,4-dichlorophenyl)-guanidine

: 1224570-47-1
N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine

Guidance literature:: In chloroform; at 100 ℃; Sealed tube;
DOI:10.1016/j.bmc.2010.12.028

Reference yield:

: 18995-48-7
N-(3,4-dichlorophenyl)cyanamide

: 1224570-47-1
N-(3,4-dichloro-phenyl)-N'-(1-isopropyl-4,5-dioxo-4,5-dihydro-1H-imidazol-2-yl)-N''-t-butoxyguanidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 18 h / Reflux

1.2: Saturated solution

2.1: chloroform / 100 °C / Sealed tube

In ethanol; chloroform;
DOI:10.1016/j.bmc.2010.12.028