benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate

Base Information

Chemical Name:benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate
CAS No.:129815-30-1
Molecular Formula:C₂₉H₄₀O₇S
Molecular Weight:532.698
Hs Code.:

Synonyms:benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate

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Chemical Property of benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate

Chemical Property:

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Technology Process of benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate

There total 3 articles about benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 6553-96-4
2,4,6-triisopropylphenylsulfonyl chloride

: 129815-29-8
(E)-(5S,6R)-5,6,7-Trihydroxy-hept-2-enoic acid benzyl ester

: 129815-30-1
benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate

Guidance literature:: With pyridine; for 24h; Ambient temperature;
DOI:10.1016/0008-6215(90)84073-4

Reference yield:

: 533-67-5
2-Deoxy-D-ribose

: 129815-30-1
benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / tetrahydrofuran / 4 h / Heating

2: 93 percent / pyridine / 24 h / Ambient temperature

With pyridine; In tetrahydrofuran;
DOI:10.1016/0008-6215(90)84073-4

Reference yield:

: 15097-38-8
(carbobenzyloxymethylene)triphenylphosphorane

: 129815-30-1
benzyl (5S,6R)-5,6-dihydroxy-7-(triisopropylbenzenesulfonyloxy)-2-heptenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / tetrahydrofuran / 4 h / Heating

2: 93 percent / pyridine / 24 h / Ambient temperature

With pyridine; In tetrahydrofuran;
DOI:10.1016/0008-6215(90)84073-4