C₆₄H₁₀₄O₁₁Si₃

Base Information

• Chemical Name: C₆₄H₁₀₄O₁₁Si₃
• CAS No.: 1187471-48-2
• Molecular Formula: C₆₄H₁₀₄O₁₁Si₃
• Molecular Weight: 1133.78
• Mol file: 1187471-48-2.mol

Synonyms:C₆₄H₁₀₄O₁₁Si₃

Chemical Property of C₆₄H₁₀₄O₁₁Si₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₆₄H₁₀₄O₁₁Si₃

There total 2 articles about C₆₄H₁₀₄O₁₁Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C64H102O10Si3 (1187471-45-9) → C64H104O11Si3 (1187471-48-2)

Guidance literature:

C₆₄H₁₀₂O₁₀Si₃; With thexylborane; In tetrahydrofuran; at -10 - 25 ℃; for 0.5h; Inert atmosphere;

With borane-THF; In tetrahydrofuran; at 25 ℃; for 1h; Further stages; Inert atmosphere;

DOI:10.1002/anie.200902029

Reference yield:

C70H109NO14SeSi3 → C64H104O11Si3 (1187471-48-2)

Guidance literature:

C₇₀H₁₀₉NO₁₄SeSi₃; With dihydrogen peroxide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With pyridine; In tetrahydrofuran; at 45 ℃; for 0.5h; Inert atmosphere;

DOI:10.1021/ja100742b

Reference yield: 93.0%

triethylsilyl chloride (994-30-9) + C64H104O11Si3 (1187471-48-2) → C70H118O11Si4 (1187471-89-1)

Guidance literature:

C₆₄H₁₀₄O₁₁Si₃; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -50 ℃; for 0.0833333h; Inert atmosphere;

triethylsilyl chloride; With triethylamine; In tetrahydrofuran; toluene; at -50 - 25 ℃; Inert atmosphere;

DOI:10.1002/anie.200902029

upstream raw materials:

C₆₄H₁₀₂O₁₀Si₃

Downstream raw materials:

C₇₀H₁₁₈O₁₁Si₄