(+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate

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Chemical Name:(+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate
CAS No.:98736-91-5
Molecular Formula:C₂₅H₂₃BrN₂O₆
Molecular Weight:527.371
Hs Code.:

Synonyms:(+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate

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Chemical Property of (+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate

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Technology Process of (+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate

There total 4 articles about (+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98736-90-4
(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4(1H,3H)-pyrimidinedione dibenzoate

: 98736-91-5
(+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; for 1h; Heating; Irradiation;
DOI:10.1021/jm00151a013

Reference yield:

: 61849-27-2
(+/-)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-5-methyl-2,4-(1H,3H)pyrimidinedione

: 98736-91-5
(+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / pyridine / 2-methyl-tetrahydro-furan / 70 h / 58 °C

2: 78 percent / aq. HCl / ethanol / 24 h / Heating

3: 99 percent / N-bromosuccinimide / CCl₄ / 1 h / Heating; Irradiation

With pyridine; hydrogenchloride; N-Bromosuccinimide; In 2-methyltetrahydrofuran; tetrachloromethane; ethanol;
DOI:10.1021/jm00151a013

Reference yield:

: 98-88-4
benzoyl chloride

: 98736-91-5
(+/-)-5-(bromomethyl)-1-<(1α,3β,4α)-3-hydroxy-4-(hydroxymethyl)cyclopentyl>-2,4(1H,3H)-pyrimidinedione dibenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / pyridine / 2-methyl-tetrahydro-furan / 70 h / 58 °C

2: 78 percent / aq. HCl / ethanol / 24 h / Heating

3: 99 percent / N-bromosuccinimide / CCl₄ / 1 h / Heating; Irradiation

With pyridine; hydrogenchloride; N-Bromosuccinimide; In 2-methyltetrahydrofuran; tetrachloromethane; ethanol;
DOI:10.1021/jm00151a013