endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.0^2,6]dec-8-ene-10-carboxylic acid methyl ester

Base Information

• Chemical Name: endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.0^2,6]dec-8-ene-10-carboxylic acid methyl ester
• CAS No.: 933775-85-0
• Molecular Formula: C₁₆H₁₄N₂O₄
• Molecular Weight: 298.298

Synonyms:endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.0^2,6]dec-8-ene-10-carboxylic acid methyl ester

Chemical Property of endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.0^2,6]dec-8-ene-10-carboxylic acid methyl ester

Chemical Property:

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Technology Process of endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.0^2,6]dec-8-ene-10-carboxylic acid methyl ester

There total 1 articles about endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.0^2,6]dec-8-ene-10-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-phenyl-maleimide (941-69-5) + methyl 1H-pyrrole-1-carboxylate (4277-63-8) → endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.02,6]dec-8-ene-10-carboxylic acid methyl ester (933775-85-0)

Guidance literature:

In dichloromethane; at 25 ℃; under 10500800 Torr;

DOI:10.3390/11080603

Reference yield: 72.0%

endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.02,6]dec-8-ene-10-carboxylic acid methyl ester (933775-85-0) + 1-Chloro-4-iodobenzene (637-87-6) → endo-(8-exo-4-chlorophenyl)-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.02,6]decane-10-carboxylic acid methyl ester

Guidance literature:

With formic acid; triphenyl-arsane; triethylamine; palladium diacetate; Heating;

DOI:10.3390/11080603

Reference yield: 58.0%

endo-3,5-dioxo-4-phenyl-4,10-diazatricyclo[5.2.1.02,6]dec-8-ene-10-carboxylic acid methyl ester (933775-85-0) + 2-Iodothiophene (3437-95-4,149762-92-5) → endo-3,5-dioxo-4-phenyl-8-exo-(2-thienyl)-4,10-diazatricyclo[5.2.1.02,6]decane-10-carboxylic acid methyl ester

Guidance literature:

With formic acid; triphenyl-arsane; triethylamine; palladium diacetate; Heating;

DOI:10.3390/11080603

upstream raw materials:

N-phenyl-maleimide

methyl 1H-pyrrole-1-carboxylate

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