5-(pyridin-2-ylmethyl)aminoisophthalic acid

Base Information

Chemical Name:5-(pyridin-2-ylmethyl)aminoisophthalic acid
CAS No.:1345821-81-9
Molecular Formula:C₁₄H₁₂N₂O₄
Molecular Weight:272.26
Hs Code.:

Synonyms:5-(pyridin-2-ylmethyl)aminoisophthalic acid

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Chemical Property of 5-(pyridin-2-ylmethyl)aminoisophthalic acid

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Technology Process of 5-(pyridin-2-ylmethyl)aminoisophthalic acid

There total 1 articles about 5-(pyridin-2-ylmethyl)aminoisophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.9%

: 1121-60-4
pyridine-2-carbaldehyde

: 99-31-0
5-aminoisophthalic acid

: 1345821-81-9
5-(pyridin-2-ylmethyl)aminoisophthalic acid

Guidance literature:: pyridine-2-carbaldehyde; 5-aminoisophthalic acid; With triethylamine; In methanol; for 10h;

With sodium tetrahydroborate; In methanol; at 4 ℃; for 10h;

With acetic acid; In water; pH=5 - 6;
DOI:10.1002/zaac.201100160

Reference yield: 65.9%

: zinc(II) nitrate hexahydrate

: 1345821-81-9
5-(pyridin-2-ylmethyl)aminoisophthalic acid

: 7732-18-5
water

: 1345821-76-2
[Zn(5-pyridin-2-ylmethyl)aminoisophthalate)(H₂O)]n

Guidance literature:: With NaOH; In water; High Pressure; stirred in air for 10 min; transferred to stainless steel container, heated at 180°C for 3 d; cooled to room temp.; isolated by filtration, washed with water and EtON several times; elem. anal.;
DOI:10.1002/zaac.201100160

Reference yield: 57.9%

: cobalt(II) nitrate hexahydrate

: 1345821-81-9
5-(pyridin-2-ylmethyl)aminoisophthalic acid

: 7732-18-5
water

: 1345821-78-4,1370584-94-3
[Co(5-pyridin-2-ylmethyl)aminoisophthalate)(H₂O)]n

Guidance literature:: With NaOH; In water; High Pressure; stirred in air for 10 min; transferred to stainless steel container, heated at 180°C for 3 d; cooled to room temp.; isolated by filtration, washed with water and EtON several times; elem. anal.;
DOI:10.1002/zaac.201100160