trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester
CAS No.:269405-64-3
Molecular Formula:C₂₃H₁₇F₃N₂O₅S
Molecular Weight:490.46
Hs Code.:

Synonyms:trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

Suppliers and Price of trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

There total 2 articles about trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 269405-61-0
acetic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

: 269405-64-3
trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. K₂CO₃ / methanol / 3 h / 20 °C

2: 0.4 g / Et₃N / CH₂Cl₂ / 12 h

With potassium carbonate; triethylamine; In methanol; dichloromethane; 1: Deacetylation / 2: Substitution;
DOI:10.1021/jo9915729

Reference yield:

: 145100-51-2
N-(5-chloropyridin-2-yl)-1,1,1-trifluoro-N-[(trifluoromethyl)sulphonyl]methanesulphonamide

: 1025809-63-5
4-benzoyl-9-hydroxy-7-methyl-4,5,5a,7-tetrahydro-6H-indolo[4,3-fg]quinolin-8-one

: 269405-64-3
trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

Guidance literature:: With triethylamine; In dichloromethane; for 12h;
DOI:10.1021/jo9915729

Reference yield: 73.0%

: 594-27-4
tetramethylstannane

: 269405-64-3
trifluoromethanesulfonic acid 4-benzoyl-7-methyl-8-oxo-4,5,5a,6,7,8-hexahydroindolo[4,3-fg]quinolin-9-yl ester

: 269405-65-4
4-benzoyl-7,8-dimethyl-4,5,5a,7-tetrahydro-6H-indolo[4,3-fg]quinolin-8-one

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; lithium chloride; In N,N-dimethyl-formamide; at 100 ℃; for 2h;
DOI:10.1021/jo9915729