Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester

Base Information

• Chemical Name: Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester
• CAS No.: 129152-10-9
• Molecular Formula: C₂₀H₂₄N₂O₂S
• Molecular Weight: 356.489

Synonyms:Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester

Chemical Property of Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester

There total 2 articles about Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Cyclohepten-1-one (1121-66-0) → Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester (129152-10-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Mg

With magnesium;

DOI:10.1021/jo00305a001

Reference yield:

3-(3-Phenyl-propyl)-cyclohept-2-enone + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester (129152-10-9)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00305a001

Reference yield: 58.0%

Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester (129152-10-9) → (3aR,8aR)-1-Phenyl-octahydro-azulen-3a-ol (129152-15-4,129152-20-1)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;

DOI:10.1021/jo00305a001

upstream raw materials:

1,1'-Thiocarbonyldiimidazole

2-Cyclohepten-1-one

Downstream raw materials:

(3aR,8aR)-1-Phenyl-octahydro-azulen-3a-ol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 129152-10-9 Imidazole-1-carbothioic acid O-[(1S,2S,7S)-7-(3-phenyl-propyl)-8-oxa-bicyclo[5.1.0]oct-2-yl] ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send