1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole

Base Information

Chemical Name:1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole
CAS No.:472999-07-8
Molecular Formula:C₂₀H₂₃N₃O₅S
Molecular Weight:417.486
Hs Code.:

Synonyms:1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole

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Chemical Property of 1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole

Chemical Property:

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Technology Process of 1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole

There total 7 articles about 1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3288-80-0
N,N,N-trimethylhydrazinium iodide

: 472999-05-6
1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

: 472999-07-8
1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole

Guidance literature:: With sodium isopropylate; In dimethyl sulfoxide; at 20 ℃; for 4h;
DOI:10.1081/SCC-120003645

Reference yield:

: 118-96-7
2,4,6-Trinitrotoluene

: 472999-07-8
1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole

Guidance literature:: Multi-step reaction with 7 steps

1.1: K₂CO₃; NMP

2.1: H₂O₂; acetic acid / Heating

3.1: 83 percent / piperidine / benzene / Heating

4.1: NaN₃ / dimethylformamide / 6 h / 20 °C

5.1: ethane-1,2-diol / 150 - 170 °C

6.1: iPrONa / dimethylformamide / 0.5 h / 20 °C

6.2: 95 percent / dimethylformamide / 4 h / 20 - 80 °C

7.1: 90 percent / iPrONa / dimethylsulfoxide / 4 h / 20 °C

With piperidine; 1-methyl-pyrrolidin-2-one; sodium azide; dihydrogen peroxide; sodium isopropylate; potassium carbonate; acetic acid; In ethylene glycol; dimethyl sulfoxide; N,N-dimethyl-formamide; benzene;
DOI:10.1081/SCC-120003645

Reference yield:

: 367924-99-0
1-isobutylsulfanyl-2-methyl-3,5-dinitro-benzene

: 472999-07-8
1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitro-7-aminoindole

Guidance literature:: Multi-step reaction with 6 steps

1.1: H₂O₂; acetic acid / Heating

2.1: 83 percent / piperidine / benzene / Heating

3.1: NaN₃ / dimethylformamide / 6 h / 20 °C

4.1: ethane-1,2-diol / 150 - 170 °C

5.1: iPrONa / dimethylformamide / 0.5 h / 20 °C

5.2: 95 percent / dimethylformamide / 4 h / 20 - 80 °C

6.1: 90 percent / iPrONa / dimethylsulfoxide / 4 h / 20 °C

With piperidine; sodium azide; dihydrogen peroxide; sodium isopropylate; acetic acid; In ethylene glycol; dimethyl sulfoxide; N,N-dimethyl-formamide; benzene;
DOI:10.1081/SCC-120003645