1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

Base Information

Chemical Name:1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole
CAS No.:472999-05-6
Molecular Formula:C₂₀H₂₂N₂O₅S
Molecular Weight:402.471
Hs Code.:

Synonyms:1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

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Chemical Property of 1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

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Technology Process of 1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

There total 6 articles about 1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 329059-94-1
2-(4-methoxy-phenyl)-4-(2-methyl-propane-1-sulfonyl)-6-nitro-1H-indole

: 74-88-4
methyl iodide

: 472999-05-6
1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

Guidance literature:: 2-(4-methoxy-phenyl)-4-(2-methyl-propane-1-sulfonyl)-6-nitro-1H-indole; With sodium isopropylate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; at 20 - 80 ℃; for 4h;
DOI:10.1081/SCC-120003645

Reference yield:

: 118-96-7
2,4,6-Trinitrotoluene

: 472999-05-6
1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

Guidance literature:: Multi-step reaction with 6 steps

1.1: K₂CO₃; NMP

2.1: H₂O₂; acetic acid / Heating

3.1: 83 percent / piperidine / benzene / Heating

4.1: NaN₃ / dimethylformamide / 6 h / 20 °C

5.1: ethane-1,2-diol / 150 - 170 °C

6.1: iPrONa / dimethylformamide / 0.5 h / 20 °C

6.2: 95 percent / dimethylformamide / 4 h / 20 - 80 °C

With piperidine; 1-methyl-pyrrolidin-2-one; sodium azide; dihydrogen peroxide; sodium isopropylate; potassium carbonate; acetic acid; In ethylene glycol; N,N-dimethyl-formamide; benzene;
DOI:10.1081/SCC-120003645

Reference yield:

: 367925-10-8
2-methyl-1-(2-methyl-propane-1-sulfonyl)-3,5-dinitro-benzene

: 472999-05-6
1-methyl-2-para-methoxyphenyl-4-isobutylsulphonyl-6-nitroindole

Guidance literature:: Multi-step reaction with 4 steps

1.1: 83 percent / piperidine / benzene / Heating

2.1: NaN₃ / dimethylformamide / 6 h / 20 °C

3.1: ethane-1,2-diol / 150 - 170 °C

4.1: iPrONa / dimethylformamide / 0.5 h / 20 °C

4.2: 95 percent / dimethylformamide / 4 h / 20 - 80 °C

With piperidine; sodium azide; sodium isopropylate; In ethylene glycol; N,N-dimethyl-formamide; benzene;
DOI:10.1081/SCC-120003645