C₂₆H₃₆O₅Si

Base Information

Chemical Name:C₂₆H₃₆O₅Si
CAS No.:1431370-75-0
Molecular Formula:C₂₆H₃₆O₅Si
Molecular Weight:456.654
Hs Code.:

C<sub>26</sub>H<sub>36</sub>O<sub>5</sub>Si

Synonyms:C₂₆H₃₆O₅Si

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Chemical Property of C₂₆H₃₆O₅Si

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Technology Process of C₂₆H₃₆O₅Si

There total 1 articles about C₂₆H₃₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1449125-95-4,816422-95-4
C₁₀H₁₈O₅

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1431370-75-0
C₂₆H₃₆O₅Si

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 25 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol400931p

Reference yield:

: 1431370-75-0
C₂₆H₃₆O₅Si

: 100-39-0
benzyl bromide

: 1449125-96-5
C₄₀H₄₈O₅Si

Guidance literature:: C₂₆H₃₆O₅Si; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h; Inert atmosphere;

benzyl bromide; at 0 - 25 ℃; for 2h;
DOI:10.1021/ol400931p

Reference yield:

: 1431370-75-0
C₂₆H₃₆O₅Si

: 1431370-74-9
C₄₃H₄₈O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C / Inert atmosphere

1.2: 2 h / 0 - 25 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 25 °C / Inert atmosphere

3.1: gold(III) chloride / dichloromethane / 2 h / 25 °C / Molecular sieve; Inert atmosphere

4.1: sodium methylate / methanol / 2 h / 25 °C / Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 2 h / 25 °C / Inert atmosphere

With gold(III) chloride; tetrabutyl ammonium fluoride; sodium methylate; sodium hydride; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil; 5.1: |Dess-Martin Oxidation;
DOI:10.1021/ol400931p