tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate

Base Information

Chemical Name:tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate
CAS No.:1310343-27-1
Molecular Formula:C₂₂H₂₇BrN₂O₂
Molecular Weight:431.373
Hs Code.:

Synonyms:tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate

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Chemical Property of tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate

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Technology Process of tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate

There total 6 articles about tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 478672-70-7
C₁₂H₁₅BrN₂O₂

: 1310343-27-1
tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium cyanoborohydride; acetic acid / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

1.2: 1.5 h / 60 °C / Inert atmosphere

2.1: benzene / 26 h / Inert atmosphere; Reflux

3.1: diethyl ether / 0 - 20 °C / Inert atmosphere

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; diethyl ether; benzene; 3.1: Grignard reaction;
DOI:10.1021/ol201123b

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 1310343-27-1
tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

2.1: sodium cyanoborohydride; acetic acid / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

2.2: 1.5 h / 60 °C / Inert atmosphere

3.1: benzene / 26 h / Inert atmosphere; Reflux

4.1: diethyl ether / 0 - 20 °C / Inert atmosphere

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; diethyl ether; benzene; 4.1: Grignard reaction;
DOI:10.1021/ol201123b

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1310343-27-1
tert-butyl 2-(2-bromobenzyl)-2-(1-phenylbut-3-en-1-yl)hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 18 h / 20 °C / Inert atmosphere

2.1: sodium cyanoborohydride; acetic acid / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

2.2: 1.5 h / 60 °C / Inert atmosphere

3.1: benzene / 26 h / Inert atmosphere; Reflux

4.1: diethyl ether / 0 - 20 °C / Inert atmosphere

With sodium cyanoborohydride; acetic acid; In tetrahydrofuran; diethyl ether; benzene; 4.1: Grignard reaction;
DOI:10.1021/ol201123b