Technology Process of C63H76O3
There total 4 articles about C63H76O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C61H76O4;
With
acetyl chloride;
Inert atmosphere;
acetylenemagnesium bromide;
In
tetrahydrofuran; toluene;
Inert atmosphere;
DOI:10.1002/ejoc.201200655
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetone / Reflux
2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere
2.2: 20 °C / Inert atmosphere
3.1: acetyl chloride / Inert atmosphere
3.2: Inert atmosphere
With
n-butyllithium; potassium carbonate; acetyl chloride;
In
tetrahydrofuran; hexane; acetone;
DOI:10.1002/ejoc.201200655
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: acetyl chloride / Inert atmosphere
2.2: Inert atmosphere
With
n-butyllithium; acetyl chloride;
In
tetrahydrofuran; hexane;
DOI:10.1002/ejoc.201200655