N₄-tert-butyl-N₂-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine

Base Information

• Chemical Name: N₄-tert-butyl-N₂-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine
• CAS No.: 1215103-32-4
• Molecular Formula: C₂₅H₃₀N₄
• Molecular Weight: 386.54

Synonyms:N₄-tert-butyl-N₂-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine

Chemical Property of N₄-tert-butyl-N₂-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine

Chemical Property:

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Technology Process of N₄-tert-butyl-N₂-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine

There total 1 articles about N₄-tert-butyl-N₂-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester (1215104-15-6) → N4-tert-butyl-N2-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine (1215103-32-4)

Guidance literature:

methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester; With lithium aluminium tetrahydride; In tetrahydrofuran; at 35 ℃; for 18h; Cooling with ice-water bath; Inert atmosphere;

With water; sodium hydroxide; In tetrahydrofuran; Cooling with ice;

upstream raw materials:

methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester

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