methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester

Base Information

Chemical Name:methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester
CAS No.:1215104-15-6
Molecular Formula:C₂₆H₃₂N₄O₃S
Molecular Weight:480.631
Hs Code.:

Synonyms:methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester

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Technology Process of methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester

There total 1 articles about methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1215103-21-1
{1-[4-(4-tert-Butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl}-cyclobutyl}-methanol

: 124-63-0
methanesulfonyl chloride

: 1215104-15-6
methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 35 ℃; Inert atmosphere; Cooling with ice-water bath;

Reference yield: 45.0%

: 1215104-15-6
methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester

: 1215103-32-4
N₄-tert-butyl-N₂-[4-(1-methyl-cyclobutyl)-phenyl]-6-phenyl-pyrimidine-2,4-diamine

Guidance literature:: methanesulfonic acid 1-[4-(4-tert-butylamino-6-phenyl-pyrimidin-2-ylamino)-phenyl]-cyclobutylmethyl ester; With lithium aluminium tetrahydride; In tetrahydrofuran; at 35 ℃; for 18h; Cooling with ice-water bath; Inert atmosphere;

With water; sodium hydroxide; In tetrahydrofuran; Cooling with ice;