3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

Base Information

Chemical Name:3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester
CAS No.:1353002-80-8
Molecular Formula:C₄₃H₃₃Cl₂F₅O₁₁
Molecular Weight:891.626
Hs Code.:

3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

Synonyms:3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

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Chemical Property of 3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

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Technology Process of 3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

There total 4 articles about 3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-chloro-4-methoxybenzene-1,3-diol

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 22651-87-2
cyclohexanecarboxylic acid anhydride

: 538-75-0
dicyclohexyl-carbodiimide

: 552-30-7,145253-53-8
trimellitic Anhydride

: 1353002-81-9
3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-6-carboxylic acid pentafluorophenyl ester

: 1353002-80-8
3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

: 2387-23-7
1,3-Dicyclohexylurea

Guidance literature:: 2-chloro-4-methoxybenzene-1,3-diol; trimellitic Anhydride; With methanesulfonic acid; tin(IV) chloride; at 40 ℃; for 6h;

cyclohexanecarboxylic acid anhydride; With pyridine; at 70 ℃; for 1h;

2,3,4,5,6-pentafluorophenol; dicyclohexyl-carbodiimide; In ethyl acetate; at 20 ℃; for 2h;
DOI:10.1021/jo202229t

Reference yield:

: 621-59-0
isovanillin

: 1353002-80-8
3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: chlorine / chloroform / 2.5 h

2.1: selenium(IV) oxide; dihydrogen peroxide / dichloromethane; water / 48 h / 20 °C

3.1: hydrogenchloride; methanol / 0.5 h / 20 °C

4.1: methanesulfonic acid; tin(IV) chloride / 6 h / 40 °C

4.2: 1 h / 70 °C

4.3: 2 h / 20 °C

With hydrogenchloride; methanol; selenium(IV) oxide; methanesulfonic acid; dihydrogen peroxide; chlorine; tin(IV) chloride; In dichloromethane; chloroform; water;
DOI:10.1021/jo202229t

Reference yield:

: 37687-57-3
2-chloro-3-hydroxy-4-methoxybenzaldehyde

: 1353002-80-8
3',6'-bis(cyclohexylcarbonyloxy)-4',5'-dichloro-2',7'-dimethoxy-3-oxospiro[isobenzofuran-1(3H),9'-[9H]xanthene]-5-carboxylic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: selenium(IV) oxide; dihydrogen peroxide / dichloromethane; water / 48 h / 20 °C

2.1: hydrogenchloride; methanol / 0.5 h / 20 °C

3.1: methanesulfonic acid; tin(IV) chloride / 6 h / 40 °C

3.2: 1 h / 70 °C

3.3: 2 h / 20 °C

With hydrogenchloride; methanol; selenium(IV) oxide; methanesulfonic acid; dihydrogen peroxide; tin(IV) chloride; In dichloromethane; water;
DOI:10.1021/jo202229t