4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

Base Information

Chemical Name:4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine
CAS No.:726191-64-6
Molecular Formula:C₃₆H₄₂N₂O₈
Molecular Weight:630.738
Hs Code.:

Synonyms:4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

Suppliers and Price of 4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

There total 3 articles about 4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 24324-17-2
9-Fluorenylmethanol

: 1026823-88-0
4-(N,N,N-tris(Boc))hydrazinobenzoic acid

: 726191-64-6
4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 25 ℃; for 48h;
DOI:10.1021/jo049830b

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 726191-64-6
4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / tetrahydrofuran; dimethylformamide / 4 h / 60 °C

2: 43 percent / DCC; DMAP / CH₂Cl₂ / 48 h / 25 °C

With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo049830b

Reference yield:

: 619-67-0
4-Hydrazinobenzoic acid

: 726191-64-6
4-(9-fluorenylmethyloxycarbonyl)[N,N,N-tris(tert-butyloxycarbonyl)]phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: DMAP / tetrahydrofuran; dimethylformamide / 4 h / 60 °C

2: 43 percent / DCC; DMAP / CH₂Cl₂ / 48 h / 25 °C

With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo049830b