(S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate

Base Information

Chemical Name:(S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate
CAS No.:866603-21-6
Molecular Formula:C₄₂H₄₀O₈
Molecular Weight:672.775
Hs Code.:

Synonyms:(S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate

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Chemical Property of (S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate

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Technology Process of (S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate

There total 8 articles about (S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 866603-20-5
(S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-hydroxybenzoate

: 1486-51-7
p-(benzyloxy)benzoic acid

: 866603-21-6
(S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1039/b419479a

Reference yield:

: 252011-73-7
4-((S)-1-Methyl-heptyloxy)-benzoic acid 4-hydroxy-phenyl ester

: 866603-21-6
(S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / N,N'-dicyclohexylcarbodiimide; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 12 h / 20 °C

2: 85 percent / H₂ / Pd/C / dioxane / 50 °C

3: 70 percent / N,N'-dicyclohexylcarbodiimide; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 12 h / 20 °C

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; dichloromethane;
DOI:10.1039/b419479a

Reference yield:

: 110482-80-9
4-((S)-1-Methyl-heptyloxy)-benzoic acid 4-benzyloxy-phenyl ester

: 866603-21-6
(S)-(+)-4-[4-(1-methylheptyloxy)benzoyloxy]phenyl 3-(4-benzyloxybenzoyloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / dioxane

2: 72 percent / N,N'-dicyclohexylcarbodiimide; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 12 h / 20 °C

3: 85 percent / H₂ / Pd/C / dioxane / 50 °C

4: 70 percent / N,N'-dicyclohexylcarbodiimide; 4-(N,N-dimethylamino)pyridine / CH₂Cl₂ / 12 h / 20 °C

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; dichloromethane;
DOI:10.1039/b419479a