N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea

Base Information

Chemical Name:N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea
CAS No.:96913-34-7
Molecular Formula:C₁₇H₁₇ClN₄O₂S
Molecular Weight:376.867
Hs Code.:

Synonyms:N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea

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Chemical Property of N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea

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Technology Process of N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea

There total 5 articles about N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 96898-67-8
5-(2-Chloro-4-isothiocyanato-phenyl)-3-furan-2-yl-[1,2,4]oxadiazole

: 109-89-7
diethylamine

: 96913-34-7
N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea

Guidance literature:: Ambient temperature;
DOI:10.1021/jm00147a019

Reference yield:

: 7073-36-1
2-chloro-4-nitrobenzoyl chloride

: 96913-34-7
N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / BF₃*Et₂O / dioxane / Heating

2: 54 percent / H₂, conc. HCl / 10percent Pd/C / aq. ethanol / 2585.7 Torr

3: 61 percent / CaCO₃ / 1,2-dimethoxy-ethane; H₂O / 1.5 h

4: 74 percent / Ambient temperature

With hydrogenchloride; boron trifluoride diethyl etherate; hydrogen; calcium carbonate; palladium on activated charcoal; In 1,4-dioxane; 1,2-dimethoxyethane; ethanol; water;
DOI:10.1021/jm00147a019

Reference yield:

: 50892-99-4
N-hydroxyfuran-2-carboximidamide

: 96913-34-7
N'-<3-chloro-4-<3-(furanyl)-1,2,4-oxadiazol-5-yl>phenyl>-N,N-diethylthiourea

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / BF₃*Et₂O / dioxane / Heating

2: 54 percent / H₂, conc. HCl / 10percent Pd/C / aq. ethanol / 2585.7 Torr

3: 61 percent / CaCO₃ / 1,2-dimethoxy-ethane; H₂O / 1.5 h

4: 74 percent / Ambient temperature

With hydrogenchloride; boron trifluoride diethyl etherate; hydrogen; calcium carbonate; palladium on activated charcoal; In 1,4-dioxane; 1,2-dimethoxyethane; ethanol; water;
DOI:10.1021/jm00147a019