1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole

Base Information

Chemical Name:1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole
CAS No.:96938-84-0
Molecular Formula:C₁₈H₁₆ClN₃O₃
Molecular Weight:357.796
Hs Code.:

Synonyms:1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole

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Chemical Property of 1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole

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Technology Process of 1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole

There total 4 articles about 1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 5673-07-4
2,6-dimethoxytoluene

: 96938-79-3
5-Chloro-1-(phenylmethyl)-1H-1,2,3-triazole-4-carbonyl chloride

: 96938-84-0
1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole

Guidance literature:: With aluminium trichloride; In dichloromethane; for 30h; Ambient temperature;

Reference yield:

: 75020-50-7
ethyl 1-benzyl-5-chloro-1H-1,2,3-triazole-4-carboxylate

: 96938-84-0
1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / 1M aq. sodium hydroxide / 1.5 h / 85 °C

2: 1.) thionyl chloride, 2.) aluminium chloride / 1.) reflux, 2-3 h; 2.) dichloromethane, 30 h, r.t.

With sodium hydroxide; aluminium trichloride; thionyl chloride;

Reference yield:

: 15212-80-3
1-Benzyl-5-chloro-1H-1,2,3-triazole-4-carboxylic acid

: 96938-84-0
1-Benzyl-5-chloro-4-(2-hydroxy-4-methoxy-3-methylbenzoyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride, N,N-dimethylformamide / CH₂Cl₂ / 2 h / Ambient temperature

2: 52 percent / aluminium chloride / CH₂Cl₂ / 30 h / Ambient temperature

With aluminium trichloride; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;