dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

Base Information

Chemical Name:dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane
CAS No.:1403471-04-4
Molecular Formula:C₁₇H₃₇BO₂Si
Molecular Weight:312.376
Hs Code.:

Synonyms:dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

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Chemical Property of dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

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Technology Process of dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

There total 3 articles about dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 3429-76-3
trimethyl-octyl-silane

: 73183-34-3
bis(pinacol)diborane

: 1403471-04-4
dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

: methyl(octyl)bis[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

Guidance literature:: With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; potassium tert-butylate; In tert-butyl methyl ether; at 110 ℃; for 36h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.6b02917

Reference yield:

: 3429-76-3
trimethyl-octyl-silane

: 73183-34-3
bis(pinacol)diborane

: 1403471-04-4
dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

Guidance literature:: bis(pinacol)diborane; With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; In Cyclooctan; at 110 ℃; for 0.05h; Inert atmosphere;

trimethyl-octyl-silane; In Cyclooctan; at 110 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja307956w

Reference yield:

: 3429-76-3
trimethyl-octyl-silane

: 73183-34-3
bis(pinacol)diborane

: 1403471-04-4
dimethyl(octyl)[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]silane

: C₁₇H₃₇BO₂Si

Guidance literature:: In Cyclooctan; at 135 ℃; for 12h; Reagent/catalyst; Temperature; Overall yield = 78 %; Overall yield = 81 %Chromat.;
DOI:10.1021/om400900z