Technology Process of C26H23FN2O4
There total 7 articles about C26H23FN2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate;
tetra-(n-butyl)ammonium iodide;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrahydrofuran / 5.5 h / -20 - 5 °C
2: xylenes / 0.17 h / 160 °C
3: N-iodo-succinimide / tetrahydrofuran / 0.42 h / -78 °C
4: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 1 h / 85 °C
5: caesium carbonate / tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 1 h / 0 °C
With
N-iodo-succinimide; potassium carbonate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; xylenes;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-iodo-succinimide / tetrahydrofuran / 0.42 h / -78 °C
2: potassium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,2-dimethoxyethane; water / 1 h / 85 °C
3: caesium carbonate / tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 1 h / 0 °C
With
N-iodo-succinimide; potassium carbonate; caesium carbonate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetra-(n-butyl)ammonium iodide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;