C₂₇H₃₈O₆

Base Information

Chemical Name:C₂₇H₃₈O₆
CAS No.:1427005-37-5
Molecular Formula:C₂₇H₃₈O₆
Molecular Weight:458.595
Hs Code.:

C<sub>27</sub>H<sub>38</sub>O<sub>6</sub>

Synonyms:C₂₇H₃₈O₆

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Chemical Property of C₂₇H₃₈O₆

Chemical Property:

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Technology Process of C₂₇H₃₈O₆

There total 5 articles about C₂₇H₃₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1427005-36-4
C₂₇H₃₈O₆

: 1427005-37-5
C₂₇H₃₈O₆

Guidance literature:: With 18-crown-6 ether; potassium hexamethylsilazane; In toluene; at 0 - 130 ℃; for 20.5h; Time; Temperature; Inert atmosphere;
DOI:10.1021/ol4003724

Reference yield:

: 100-39-0
benzyl bromide

: 1427005-37-5
C₂₇H₃₈O₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 0.17 h / 0 °C

1.2: 4.17 h / 0 - 80 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / 100 °C / Inert atmosphere

3.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / -78 °C

3.2: 5 h / -78 °C / Inert atmosphere

4.1: 18-crown-6 ether; potassium hexamethylsilazane / toluene / 20.5 h / 0 - 130 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cerium(III) chloride; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride; In tetrahydrofuran; toluene; 3.1: |Grignard Reaction / 3.2: |Grignard Reaction / 4.1: |Oxy-Cope Rearrangement;
DOI:10.1021/ol4003724

Reference yield:

: 1427005-33-1
C₂₄H₃₁BrO₆

: 1427005-37-5
C₂₇H₃₈O₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 48 h / 100 °C / Inert atmosphere

2.1: cerium(III) chloride / tetrahydrofuran / 1.5 h / -78 °C

2.2: 5 h / -78 °C / Inert atmosphere

3.1: 18-crown-6 ether; potassium hexamethylsilazane / toluene / 20.5 h / 0 - 130 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; cerium(III) chloride; 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; toluene; 2.1: |Grignard Reaction / 2.2: |Grignard Reaction / 3.1: |Oxy-Cope Rearrangement;
DOI:10.1021/ol4003724