methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside

Base Information

Chemical Name:methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside
CAS No.:122713-81-9
Molecular Formula:C₁₅H₂₂O₅
Molecular Weight:282.337
Hs Code.:

Synonyms:methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside

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Chemical Property of methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside

Chemical Property:

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Technology Process of methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside

There total 8 articles about methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122713-75-1
methyl 2-O-allyl-α-L-fucopyranoside

: 122713-81-9
methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / dibutyltin oxide, Bu₄NI / benzene / Heating

2: 88.8 percent / NaH / diethyl ether / Heating

3: 73 percent / tributylstannane, α,α'-azodiisobutanonitrile / benzene / 0.33 h / Heating

4: 76.4 percent / KOCMe₃ / dimethylsulfoxide / 0.25 h / 100 °C

5: HgO, HgCl₂ / acetone; H₂O

With 2,2'-azobis(isobutyronitrile); potassium tert-butylate; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; mercury dichloride; mercury(II) oxide; In diethyl ether; water; dimethyl sulfoxide; acetone; benzene;
DOI:10.1016/0008-6215(89)80056-4

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 122713-81-9
methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / dibutyltin oxide, Bu₄NI / benzene / Heating

2: 88.8 percent / NaH / diethyl ether / Heating

3: 73 percent / tributylstannane, α,α'-azodiisobutanonitrile / benzene / 0.33 h / Heating

4: 76.4 percent / KOCMe₃ / dimethylsulfoxide / 0.25 h / 100 °C

5: HgO, HgCl₂ / acetone; H₂O

With 2,2'-azobis(isobutyronitrile); potassium tert-butylate; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; mercury dichloride; mercury(II) oxide; In diethyl ether; water; dimethyl sulfoxide; acetone; benzene;
DOI:10.1016/0008-6215(89)80056-4

Reference yield:

: 122713-73-9
methyl 2-O-allyl-3,4-O-isopropylidene-α-L-fucopyranoside

: 122713-81-9
methyl 4,6-dideoxy-3-O-(4-methoxybenzyl)-α-L-xylo-hexopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 88.6 percent / 60percent aq. AcOH / 1.5 h / 60 °C

2: 92 percent / dibutyltin oxide, Bu₄NI / benzene / Heating

3: 88.8 percent / NaH / diethyl ether / Heating

4: 73 percent / tributylstannane, α,α'-azodiisobutanonitrile / benzene / 0.33 h / Heating

5: 76.4 percent / KOCMe₃ / dimethylsulfoxide / 0.25 h / 100 °C

6: HgO, HgCl₂ / acetone; H₂O

With 2,2'-azobis(isobutyronitrile); potassium tert-butylate; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; acetic acid; mercury dichloride; mercury(II) oxide; In diethyl ether; water; dimethyl sulfoxide; acetone; benzene;
DOI:10.1016/0008-6215(89)80056-4